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Blog posts tagged with 'chromatography'

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Honeywell HYDRANAL™ Solvent CM for Karl Fischer Titration | Greyhound Chromatography

Honeywell Volumetry Reagents NEXTGEN Solvent

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HONEYWELL PRODUCT LISTING

HYDRANAL™ Solvent CM for Karl Fischer Titration

Medium for volumetric two-component Karl Fischer titration in non-polar substances, fats and oils (chloroform-methanol-based)
 
Honeywell Hydranal ™ Water Standards Honeywell Solvent CM Reagent for Karl Fischer Titration 

Specifications

 Advantages of Hydranal two-component reagents:

  • High titration speed
  • Ideal accuracy for small amounts of water
  • High buffer capacity
  • Exact and stable titer
  • E-type reagents: reduced toxicity compared to methanol

Specifications

Assay of Water (voL. KF) 0.005 - 0.015 Vol.%
Suitability (for KF-titration) test passed

 Properties  

Property   Value
Boiling Point/Range     60 - 65°C (1.013 hPa)
Colour     Colourless
Density     1.27 g/cm3 (20°C) 
Flashpoint     100°C
For Use with (Equipment)     KF Titration
Form     Liquid
Grade     Volumetric Two-Component KF Titration
Incompatible Materials  
  Strong Oxidising agents, Strong bases
Lower Explosion Limit     Not applicable
Melting Point/Range     No data available
Partition coefficient     No data available
Product line     HYDRANAL™
Solubility in Water     Partly miscible
Storage temperature     Ambient
Upper Explosion Limit     Not applicable
Vapor Pressure     No data available
Viscosity     No data available
pH-Value     6.0 - 7.0 (20°C)

Safety Information    

GHS Classification

                                 

 GHS08 Health Hazard          GHS06 Toxic      GHS07 Harmful

Property Value
Precautionary Statements In case of inadequate ventilation wear respiratory protection.;Wear protective gloves/protective clothing/eye protection/face protection.;Do not breathe dust/fumes/gas/mist/vapours/spray.
Hazard Class 6.1
Package Group III
UN ID UN2810

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Honeywell HYDRANAL™ Solvent E Reagent for Karl Fischer Titration | Greyhound Chromatography

Honeywell Volumetry Reagents NEXTGEN Solvent

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 HONEYWELL PRODUCT LISTING

HYDRANAL™ Solvent E Reagent for Karl Fischer Titration

Medium for volumetric two-component Karl Fischer titration (ethanol-based)
 
Synonym(s)
Ethyl Alcohol
 
Honeywell Hydranal ™ Water Standards Honeywell Solvent E reagent for Karl Fischer Titration

Specifications

Advantages of Hydranal two-component reagents:

  • High titration speed
  • Ideal accuracy for small amounts of water
  • High buffer capacity
  • Exact and stable titer
  • E-type reagents: reduced toxicity compared to methanol

 

Specifications

Assay of Water (vol. KF) 0.01 - 0.02 vol.%
Suitability (for KF-titration) test passed

Properties  

Property   Value
Boiling Point/Range     75°C (1.013 hPa)
Colour     No data available
Density     0.895 g/cm3 (20°C) 
Flashpoint     12°C
For Use with (Equipment)     KF Titration
Form     Liquid
Grade     Volumetric two-Component KF Titration
Incompatible Materials     formation of explosive gas/air mixtures
Lower Explosion Limit     No data available
Melting Point/Range     No data available
Partition coefficient     No data available
Product line     HYDRANAL™
Solubility in Water     Completely Miscible
Storage temperature     Ambient
Upper Explosion Limit     No data available
Vapor Pressure     No data available
Viscosity     No data available
pH-Value     6.6  (20°C) 

Safety Information    

GHS Classification

                                                      

    GHS08 Health Hazard          GHS05 Corrosive       GHS02 Flammable  

Property Value
Precautionary Statements Do not breathe dust/fumes/gas/mist/vapours/spray.;Wear protective gloves/protective clothing/eye protection/face protection.;In case of inadequate ventilation wear respiratory protection
Hazard Class 3
Package Group II
UN ID UN1170

 

 

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Karl Fischer Titration | Greyhound Chromatography

Karl Fisher Titration

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Karl Fisher Titration Coulometry Reagents        

Karl Fischer Titration Coulometry Reagents

Karl Fischer reagents used to determine the amount of water in an analyte by measuring the amount of electricity (in coulombs) consumed or produced during electrolysis. 

HYDRANAL™ Coulomat AG-Oven HYDRANAL™ Coulomat CG-K
HYDRANAL™ Coulomat AG-H HYDRANAL™ Coulomat AF 7
HYDRANAL™ Coulomat AK HYDRANAL™ Coulomat A
HYDRANAL™ Coulomat E HYDRANAL™ Coulomat AD
HYDRANAL™ Coulomat CG HYDRANAL™ Coulomat AG
HYDRANAL™ Coulomat Oil HYDRANAL™ Coulomat AG-F1
Karl Fisher Volumetry Reagents        

Karl Fischer Titration Volumetry Reagents

Reagents used in water determination techniques that involve measuring the volume of titrant needed to enact a change in the analyte. 

HYDRANAL™ Composite 1  HYDRANAL™ Methanol Rapid  
HYDRANAL™ Composite 2 HYDRANAL™ Methanol B
HYDRANAL™ Composite 5   HYDRANAL™ Solvent
HYDRANAL™ Composite 5 K   
HYDRANAL™ CompoSolver E    HYDRANAL™ Solvent CM
HYDRANAL™ Karl Fisher Reagent       HYDRANAL™ Solvent E
HYDRANAL™ Karl Fisher Reagent Solution A HYDRANAL™ Solvent Oil
HYDRANAL™ Karl Fischer Reagent Solution B
HYDRANAL™ KetoSolver       HYDRANAL™ Solver (Crude) Oil
HYDRANAL™ LioSolver CM   HYDRANAL™ Titrant 2
HYDRANAL™ LipoSolver MH       
HYDRANAL™ Medium K    HYDRANAL™  Titrant 5
HYDRANAL™ Methanol dry      HYDRANAL™ Working medium K
  HYDRANAL™ Working medium 5
HYDRANAL™ NEXTGEN Solvent E-F1
  
 Karl Fisher Titration Water Standards        

Karl Fischer Titration Water Standards

Reference Standards for water. Water standards are used in Karl Fisher Titration. 

HYDRANAL™ CRM Water Standard 0.1 PC HYDRANAL™ Sodium tartrate dihydrate
HYDRANAL™ CRM Water Standard 1.0 PC   HYDRANAL™ Standard 5
HYDRANAL™ CRM Water Standard Oil HYDRANAL™ Water standard 1.0
HYDRANAL™ CRM Water-in-methanol   HYDRANAL™ Water standard 10.0
HYDRANAL™ Silver sulfate solution HYDRANAL™  Water standards KF -Oven 140 - 160o
HYDRANAL™ CRM Sodium tartrate dihydrate HYDRANAL™  Water standards KF -Oven 220 - 230o
 
Karl Fisher Titration Auxillaries        

Karl Fischer Titration Auxiliaries

Associated products for Karl Fischer titration. Includes sorbents, buffer substances, Karl Fischer labware, solubilizers, and kits.

Karl Fisher Titration Next Gen Reagents        

Karl Fisher Next Gen Reagents

The next generation in Karl Fisher Titration.  Upgrade to RFID technology for automatic data transfer or use safer CMR free formulations. 

 

Honeywell Karl Fischer Titration Guide PosterDOWNLOAD THE POSTER

Honeywell Karl Fischer Titration

Register for a variety of on-demand webinars, covering all aspects of Karl Fischer Titration.

Learn to master Karl Fischer Titration      REGISTER

Karl Fischer (KF) titration is the method of choice for measuring water content in all types of substances. Although modern KF titration is fast and easy, even experienced users may not be aware of all the factors influencing accuracy and repeatability of results. Join this webinar to learn how to properly prepare your system to work with various samples and avoid common errors.


Learning Objectives of Webinar

 How to select the proper KFT method, reagents and standards for your sample.

  1. How to accurately calculate sample size, including burette volume and titer of reagent.
  2. How to avoid common errors during sample preparation & handling.
  3. How to troubleshoot for sample solubility issues, side reactions, ideal pH, stable drift.

Quality Management Of The Karl Fisher System   YOU TUBE LINK

 Karl Fischer titration is the most widely used method for water determination but requires a known amount of water, a starting point. Administering that water can be a challenge.

Maximising Solubility For Your Sample   REGISTER

Accurate Karl Fischer water determination requires the sample to release its water completely. Not all samples will be soluble in the standard media, hence, to address this issue, we will discuss different options to improve the sample solubility.

  • Find out how co-solvent additions can help improve your titrations.
  • Does your sample make you boiling mad? We’ll show you how to get even.

Join this Hydranal webinar and bring your Karl Fischer titration closer to perfection.

Tips And Tricks To Analyse Difficult Samples Using The Karl Fischer Oven Technique   REGISTER

 

Karl Fischer (KF) titration is an industry standard method for measuring water content in all types of substances. However, for various reasons some substances are not suitable for a direct Karl Fischer titration:

 

 They release their water only slowly

  • The water is released at high temperature only
  • The substances are poorly soluble in KF solvents
  • They undergo side reactions with KF reagents
  • They contaminate the titration cell or the electrodes

By using the KF oven technique, the above-mentioned problems can be avoided. This makes the KF oven technique a perfect solution for the analysis of difficult samples.

 By viewing this webinar you will learn…

  how to analyse difficult samples

  • how to properly prepare your titration system with KF oven
  • how to prepare your sample
  • how to select the optimal heating temperature
  • which reagents and which water standards you should use to obtain accurate results

After viewing this webinar you will know how to perform accurate titrations using the Karl Fischer oven technique. Additionally, the speakers will reveal tips and tricks to help you in the daily routine. The webinar will finish with live Q&A session.

 Do not hesitate and register for this webinar to benefit from the experience of the two speakers.

Achieving Best results In Water Content Determination By Karl Fisher Titration   REGISTER

The Karl Fischer titration is the most versatile and generally accepted analytical method for determining water content.  It is independent of the sample’s state of matter and is therefore suitable for the analysis of solids, liquids, and gases.  Critical to the accurate determination of water content is that the sample is soluble in the solvent mixture, the working pH of the system is not affected by the sample, and side reactions are avoided.

 This webinar will provide a brief discussion of the development and principles behind Karl Fischer analysis.  An outline of the differences between the volumetric and coulometric approaches to water determination will also be presented.  Although each method has its own advantages, the sample will typically dictate the method to be used. 

 Not only will the sample determine the Karl Fischer approach to take; it also dictates what modifications must be made to the system. To improve solubility, the addition of a co-solvent, the elevation of the system’s temperature and the addition of a homogenizer are all acceptable methods of improving sample solubility. The addition of an appropriate buffer may be required to maintain proper pH control. Problematic functional groups and the specialty reagents that allow for their analysis will be discussed. In addition, the Karl Fischer Oven will be discussed with regard to insoluble or problematic samples.     

A brief discussion of how various standards should be used to verify that the system is functioning properly, after modification for the sample, will be covered. Questions are always welcome and will be encouraged throughout the webinar.

 

 

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Honeywell Powerpoint Presentation

 

Honeywell Product Overview

 

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Steroid Botanical Reference Materials | Extrasynthese | Greyhound Chromatography

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Extrasynthese are experts in extraction, synthesis and purification of natural substances. Their product portfolio consists of hundreds of products, after almost 30 years of research and development creating reference standards for regulatory filing, quality testing, or as substrates for early stage R&D. Download and view the Extrasynthese catalogues below listed in alphabetical order, or search via CAS or product name using the search facility. 

   

 

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Catalogue 2 Labware                         Catalogue 3 Reagents                       Catalogue 4 Bio Specialities

Catalogue 5 Chemical Synthesis                         Catalogue 6 Bio Applications                        Catalogue 7 Hematology

Catalogue 8 Stable Isotopes                          Catalogue 9 Flavors & Fragrances

 

 

 

Alkaloid Botanical Reference Materials | Extrasynthese| Greyhound Chromatography

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Extrasynthese are experts in extraction, synthesis and purification of natural substances. Their product portfolio consists of hundreds of products, after almost 30 years of research and development creating reference standards for regulatory filing, quality testing, or as substrates for early stage R&D. Download and view the Extrasynthese catalogues below listed in alphabetical order, or search via CAS or product name using the search facility. 

If you can't see what you're looking for please email sales@greyhoundchrom.com we will be happy to assist you. 

   

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Catalogue 5 Chemical Synthesis                         Catalogue 6 Bio Applications                        Catalogue 7 Hematology

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Anthocyanin Botanical Reference Material | Extrasynthese | Greyhound Chromatography

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Extrasynthese are experts in extraction, synthesis and purification of natural substances. Their product portfolio consists of hundreds of products, after almost 30 years of research and development creating reference standards for regulatory filing, quality testing, or as substrates for early stage R&D. Download and view the Extrasynthese catalogues below listed in alphabetical order, or search via CAS or product name using the search facility. 

If you don't see what you're looking for please email sales@greyhoundchrom.com we will be happy to source products for you. 

 

   

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Wellington Laboratories Catalogue Image            PFAS EBook  PFAS Environmental EBook

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Catalogue 5 Chemical Synthesis                         Catalogue 6 Bio Applications                        Catalogue 7 Hematology

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Coumarin Botanical Reference Material | Extrasynthese | Greyhound Chromatography

Extrasynthese Web Page Header

Extrasynthese are experts in extraction, synthesis and purification of natural substances. Their product portfolio consists of hundreds of products, after almost 30 years of research and development creating reference standards for regulatory filing, quality testing, or as substrates for early stage R&D. Download and view the Extrasynthese catalogues below listed in alphabetical order, or search via CAS or product name using the search facility. 

   

 

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Wellington Laboratories Catalogue Image            PFAS EBook  PFAS Environmental EBook

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Dandy Vice Brochure  Chem Service Catalogue  

Catalogue 2 Labware                         Catalogue 3 Reagents                       Catalogue 4 Bio Specialities

Catalogue 5 Chemical Synthesis                         Catalogue 6 Bio Applications                        Catalogue 7 Hematology

Catalogue 8 Stable Isotopes                          Catalogue 9 Flavors & Fragrances